5--2,4-dinitrobenzoic acid

Base Information

Chemical Name:5--2,4-dinitrobenzoic acid
CAS No.:156423-08-4
Molecular Formula:C₁₁H₁₂ClN₃O₆
Molecular Weight:317.686
Hs Code.:

5-<N-(2-chloroethyl)-N-ethylamino>-2,4-dinitrobenzoic acid

Synonyms:5--2,4-dinitrobenzoic acid

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Chemical Property of 5--2,4-dinitrobenzoic acid

Chemical Property:

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Technology Process of 5--2,4-dinitrobenzoic acid

There total 4 articles about 5--2,4-dinitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 156423-07-3
methyl 5--2,4-dinitrobenzoate

: 156423-08-4
5--2,4-dinitrobenzoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 1h; Heating;
DOI:10.1021/jm00040a009

Reference yield:

: 150272-08-5
methyl 5-chloro-2,4-dinitrobenzoate

: 156423-08-4
5--2,4-dinitrobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / dioxane / 8 h / 20 °C

2: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

3: LiCl / dimethylformamide / 0.25 h / 80 °C

4: 88 percent / aq. NaOH / methanol / 1 h / Heating

With sodium hydroxide; triethylamine; lithium chloride; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009

Reference yield:

: 156423-06-2
methyl 2,4-dinitro-5-benzoate

: 156423-08-4
5--2,4-dinitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: LiCl / dimethylformamide / 0.25 h / 80 °C

3: 88 percent / aq. NaOH / methanol / 1 h / Heating

With sodium hydroxide; triethylamine; lithium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009