(2-methylphenyl)(morpholin-4-yl)methanone

Base Information

Chemical Name:(2-methylphenyl)(morpholin-4-yl)methanone
CAS No.:22978-34-3
Molecular Formula:C12H15 N O2
Molecular Weight:205.257
Hs Code.:
Mol file:22978-34-3.mol

Synonyms:Morpholine,4-(2-methylbenzoyl)- (9CI); Morpholine, 4-o-toluoyl- (8CI); NSC 38115; NSC404586

Suppliers and Price of (2-methylphenyl)(morpholin-4-yl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (2-methylphenyl)(morpholin-4-yl)methanone

Chemical Property:

Vapor Pressure:1.61E-05mmHg at 25°C
Boiling Point:365.1°Cat760mmHg
Flash Point:174.6°C
Density:1.128g/cm³

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-methylphenyl)(morpholin-4-yl)methanone

There total 19 articles about (2-methylphenyl)(morpholin-4-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 110-91-8,99108-56-2
morpholine

: 89-95-2
2-methyl-benzyl alcohol

: 22978-34-3
(2-methyl-phenyl)-(morpholin-4-yl)methanone

Guidance literature:: 2-methyl-benzyl alcohol; With sulfuric acid; dihydrogen peroxide; sodium bromide; In 1,4-dioxane; water; at 70 ℃;

morpholine; With tert.-butylhydroperoxide; In 1,4-dioxane; at 80 ℃;
DOI:10.1039/c5ra20838f

Reference yield: 90.0%

: 110-91-8,99108-56-2
morpholine

: 87-24-1
ethyl 2-methylbenzoate

: 22978-34-3
(2-methyl-phenyl)-(morpholin-4-yl)methanone

Guidance literature:: morpholine; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 0 ℃; for 3h; Inert atmosphere;

ethyl 2-methylbenzoate; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tet.2014.03.045

Reference yield: 90.0%

: 110-91-8,99108-56-2
morpholine

: 615-37-2
ortho-methylphenyl iodide

: 201230-82-2
carbon monoxide

: 22978-34-3
(2-methyl-phenyl)-(morpholin-4-yl)methanone

Guidance literature:: With potassium carbonate; In acetonitrile; at 100 ℃; for 24h; under 760.051 Torr; Schlenk technique;
DOI:10.1039/c5cc10389d