1-(2',5'-dimethoxyphenyl)allyl acetate

Base Information

Chemical Name:1-(2',5'-dimethoxyphenyl)allyl acetate
CAS No.:1348155-56-5
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:1-(2',5'-dimethoxyphenyl)allyl acetate

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Chemical Property of 1-(2',5'-dimethoxyphenyl)allyl acetate

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Technology Process of 1-(2',5'-dimethoxyphenyl)allyl acetate

There total 2 articles about 1-(2',5'-dimethoxyphenyl)allyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 155628-88-9
1-(2',5'-dimethoxyphenyl)prop-2-en-1-ol

: 108-24-7
acetic anhydride

: 1348155-56-5
1-(2',5'-dimethoxyphenyl)allyl acetate

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201201279

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 1348155-56-5
1-(2',5'-dimethoxyphenyl)allyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / -60 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; In tetrahydrofuran;
DOI:10.1002/ejoc.201201279

Reference yield: 80.0%

: 2785-98-0
2,5-dimethoxybenzoic acid

: 1348155-56-5
1-(2',5'-dimethoxyphenyl)allyl acetate

: 74-88-4
methyl iodide

: methyl 2-(2,5-dimethoxycinnamyl)-3,6-dimethoxybenzoate

Guidance literature:: 2,5-dimethoxybenzoic acid; 1-(2',5'-dimethoxyphenyl)allyl acetate; With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere; Sealed tube;

methyl iodide; With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 50 ℃; for 2h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.8b00533