(2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester
• CAS No.: 909114-57-4
• Molecular Formula: C₂₈H₃₃BrN₄O₆S
• Molecular Weight: 633.563

Synonyms:(2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

Chemical Property of (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

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Technology Process of (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

There total 2 articles about (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,5S)-2-(2-Bromo-4-nitro-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (896734-11-5) + benzenesulfonyl chloride (98-09-9) → (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (909114-57-4)

Guidance literature:

With pyridine; In dichloromethane; at 130 ℃; for 0.333333h; microwave irradiation;

DOI:10.1021/jm051283e

Reference yield:

→ (2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (909114-57-4)

Guidance literature:

Reference yield:

(2R,5S)-2-(4-Benzenesulfonylamino-2-bromo-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester (909114-57-4) + trifluoroacetic acid (76-05-1) → N-{3-Bromo-4-[(2R,5S)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidin-2-ylmethoxy]-phenyl}-benzenesulfonamide; compound with trifluoro-acetic acid

Guidance literature:

In dichloromethane; for 4h;

DOI:10.1021/jm051283e

upstream raw materials:

(2R,5S)-2-(2-Bromo-4-nitro-phenoxymethyl)-5-((S)-2-cyano-pyrrolidine-1-carbonyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

benzenesulfonyl chloride

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