Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

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Chemical Name:Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate
CAS No.:73198-42-2
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:

Synonyms:Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

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Technology Process of Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

There total 2 articles about Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73210-16-9
(R)-2-[(1S,4S,5R)-4-Hydroxy-5-methyl-5-(tetrahydro-pyran-2-yloxymethyl)-cyclopent-2-enyl]-propionic acid

: 73198-42-2
Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 1.) Na, HMPA, 2.) Tetra-n-butylammonium iodide / 1.) a) THF, 0 deg C, 15 min, b) room temp., 1 h, 2.) 50 deg C, 3 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium; tetra-(n-butyl)ammonium iodide; In diethyl ether;
DOI:10.1021/jo01299a043

Reference yield:

: 100-39-0
benzyl bromide

: 73198-41-1
Methyl α,5-Dimethyl-4-hydroxy-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

: 73198-42-2
Methyl α,5-Dimethyl-4-(phenylmethoxy)-5-<<(tetrahydro-2H-pyran-2-yl)oxy>methyl>-2-cyclopenteneacetate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium; tetra-(n-butyl)ammonium iodide; Yield given. Multistep reaction; 1.) a) THF, 0 deg C, 15 min, b) room temp., 1 h, 2.) 50 deg C, 3 h;
DOI:10.1021/jo01299a043