(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

Base Information

Chemical Name:(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone
CAS No.:135006-49-4
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:

Synonyms:(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

Chemical Property:

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Technology Process of (4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

There total 3 articles about (4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77943-39-6
4-methyl-5-phenyloxazolidin-2-one

: 135006-49-4
(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, a) -78 deg C, 1 h, b) 25 deg C, RT

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, a) -78 deg C, 2 h, b) -20 deg C, overnight

With n-butyllithium; lithium diisopropyl amide;

Reference yield:

: 36394-07-7
5-hexenoyl chloride

: 135006-49-4
(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, a) -78 deg C, 1 h, b) 25 deg C, RT

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, a) -78 deg C, 2 h, b) -20 deg C, overnight

With n-butyllithium; lithium diisopropyl amide;

Reference yield:

: 135006-48-3
(4R,5S)-(+)-3-(1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

: 74-88-4
methyl iodide

: 135006-49-4
(4R,5S)-(+)-3-((2R)-2-methyl-1-oxo-5-hexenyl)-4-methyl-5-phenyloxazolidone

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, a) -78 deg C, 2 h, b) -20 deg C, overnight;