(R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate

Base Information

• Chemical Name: (R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate
• CAS No.: 1012369-57-1
• Molecular Formula: C₁₉H₂₉NO₅
• Molecular Weight: 351.443

Synonyms:(R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate

Chemical Property of (R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate

Chemical Property:

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Technology Process of (R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate

There total 1 articles about (R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-tert-butyl 4-[(allyloxy)carbonyl]-4-diazo-1-cyclohexyl-3-oxobutylcarbamate (1012369-46-8) → (R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate (1012369-57-1) + (S)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate

Guidance literature:

In dichloromethane-d2; at 35 ℃; for 0.5h; Title compound not separated from byproducts.;

DOI:10.1021/jo702275a

Reference yield:

(R)-1-tert-butyl 3-allyl 5-cyclohexyl-2-oxopyrrolidine-1,3-dicarboxylate (1012369-57-1) → (R)-tert-butyl 2-cyclohexyl-5-oxopyrrolidine-1-carboxylate (1012369-67-3)

Guidance literature:

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo702275a

upstream raw materials:

(R)-tert-butyl 4-[(allyloxy)carbonyl]-4-diazo-1-cyclohexyl-3-oxobutylcarbamate

Downstream raw materials:

(R)-tert-butyl 2-cyclohexyl-5-oxopyrrolidine-1-carboxylate

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