N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

Base Information

Chemical Name:N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine
CAS No.:170229-85-3
Molecular Formula:C₁₆H₂₅N₃O₅
Molecular Weight:339.392
Hs Code.:

Synonyms:N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

Chemical Property:

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Technology Process of N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

There total 3 articles about N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 170229-84-2
N,N-dimethyl-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

: 170229-85-3
N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

Guidance literature:: With triethylamine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1021/jm970457s

Reference yield:

: 170229-83-1
N,N-dimethyl-N'-(2-methoxyphenyl)ethylenediamine

: 170229-85-3
N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / conc. H₂SO₄, KNO₃ / H₂O / 4 h / Ambient temperature

2: 39 percent / Et₃N / CH₂Cl₂ / 24 h / Ambient temperature

With sulfuric acid; potassium nitrate; triethylamine; In dichloromethane; water;
DOI:10.1021/jm970457s

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 170229-85-3
N,N-dimethyl-N'-(tert-butyloxycarbonyl)-N'-(2-methoxy-5-nitrophenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / Na₂CO₃ / ethanol / 7 h / Heating

2: 49 percent / conc. H₂SO₄, KNO₃ / H₂O / 4 h / Ambient temperature

3: 39 percent / Et₃N / CH₂Cl₂ / 24 h / Ambient temperature

With sulfuric acid; sodium carbonate; potassium nitrate; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1021/jm970457s