[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Base Information

Chemical Name:[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine
CAS No.:130934-13-3
Molecular Formula:C₁₇H₁₈F₃N₅OS
Molecular Weight:397.424
Hs Code.:

Synonyms:[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

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Chemical Property of [8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

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Technology Process of [8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

There total 4 articles about [8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130934-12-2
Dimethyl-[9-(4-methyl-benzyl)-8-methylsulfanyl-2-trifluoromethyl-9H-purin-6-yl]-amine

: 130934-13-3
[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

: 130934-14-4
[8-Methanesulfonyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: With dihydrogen peroxide; acetic anhydride; In acetic acid; for 20h;
DOI:10.1021/jm00105a023

Reference yield:

: 131719-97-6
8-bromo-6-(dimethylamino)-2-(trifluoromethyl)-9H-purine

: 130934-13-3
[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / potassium carbonate / dimethylformamide / 16 h / Ambient temperature

2: 30 percent / ethanol / 20 h / Heating

3: toluene / 1 h / Heating

4: 50 percent / acetic anhydride, 30percent hydrogen peroxide / acetic acid / 20 h

With dihydrogen peroxide; acetic anhydride; potassium carbonate; In ethanol; acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00105a023

Reference yield:

: 130934-04-2
[8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

: 130934-13-3
[8-Methanesulfinyl-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / ethanol / 20 h / Heating

2: toluene / 1 h / Heating

3: 50 percent / acetic anhydride, 30percent hydrogen peroxide / acetic acid / 20 h

With dihydrogen peroxide; acetic anhydride; In ethanol; acetic acid; toluene;
DOI:10.1021/jm00105a023