[8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Base Information

• Chemical Name: [8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine
• CAS No.: 130934-04-2
• Molecular Formula: C₁₆H₁₅BrF₃N₅
• Molecular Weight: 414.228

Synonyms:[8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

Chemical Property of [8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

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Technology Process of [8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

There total 1 articles about [8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

8-bromo-6-(dimethylamino)-2-(trifluoromethyl)-9H-purine (131719-97-6) + 4-Methylbenzyl bromide (104-81-4) → [8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine (130934-04-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

DOI:10.1021/jm00105a023

Reference yield: 82.0%

[8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine (130934-04-2) + dimethyl amine (124-40-3) → 6,8-bis(dimethylamino)-9-(4-methylbenzyl)-2-(trifluoromethyl)-9H-purine (130934-07-5)

Guidance literature:

In ethanol; for 40h; Heating;

DOI:10.1021/jm00105a023

Reference yield: 78.0%

[8-Bromo-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine (130934-04-2) → 6-Dimethylamino-9-(4-methyl-benzyl)-2-trifluoromethyl-7,9-dihydro-purin-8-one (130934-16-6)

Guidance literature:

With sodium acetate; acetic acid; for 64h; Heating;

DOI:10.1021/jm00105a023

upstream raw materials:

8-bromo-6-(dimethylamino)-2-(trifluoromethyl)-9H-purine

4-Methylbenzyl bromide

Downstream raw materials:

[8-Methoxy-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-6-yl]-dimethyl-amine

6-Dimethylamino-9-(4-methyl-benzyl)-2-trifluoromethyl-7,9-dihydro-purin-8-one

8-amino-6-(dimethylamino)-9-(4-methylbenzyl)-2-(trifluoromethyl)-9H-purine

2-[6-Dimethylamino-9-(4-methyl-benzyl)-2-trifluoromethyl-9H-purin-8-ylamino]-ethanol

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