dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside
CAS No.:1616628-00-2
Molecular Formula:C₂₈H₄₀Cl₃NO₈Si
Molecular Weight:653.072
Hs Code.:

Synonyms:dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

There total 5 articles about dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616627-99-6
dimethylthexylsilyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1616628-00-2
dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 3h;
DOI:10.1016/j.carres.2014.05.007

Reference yield:

: 1616627-97-4
dimethylthexylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

: 1616628-00-2
dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate; methanol / 12 h

2: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

3: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h

With methanol; dmap; sodium methylate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2014.05.007

Reference yield:

: 219693-02-4
1,3,4,6-tetra-O-acetyl-2-deoxy-2-trichloroacetamido-α/β-D-glucopyranose

: 1616628-00-2
dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: benzylamine / tetrahydrofuran / 6 h

2: 1H-imidazole / dichloromethane / 24 h

3: sodium methylate; methanol / 12 h

4: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

5: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3 h

With 1H-imidazole; methanol; dmap; sodium methylate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; benzylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2014.05.007