(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

Base Information

Chemical Name:(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester
CAS No.:881011-62-7
Molecular Formula:C₂₀H₂₃NO₆S
Molecular Weight:405.472
Hs Code.:

Synonyms:(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

Chemical Property:

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Technology Process of (2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

There total 5 articles about (2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 881011-58-1
3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-2-oxo-propionic acid tert-butyl ester

: 881011-62-7
(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

: (2S,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

: (2R,3S)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

Guidance literature:: With D-glucose; magnesium sulfate; calcium carbonate; bakers' yeast; In phosphate buffer; at 35 ℃; for 144h; Title compound not separated from byproducts;
DOI:10.3987/COM-05-S(K)57

Reference yield:

: 955961-39-4
tert-butyl 3-chloro-3-(4-methoxyphenyl)-2-oxopropionate

: 881011-62-7
(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 °C

2: glucose; MgSO₄; CaCO₃ / bakers' yeast / aq. phosphate buffer / 144 h / 35 °C

With D-glucose; magnesium sulfate; calcium carbonate; bakers' yeast; In phosphate buffer; toluene;
DOI:10.3987/COM-05-S(K)57

Reference yield:

: 49653-47-6
tert-butyl 2,2-dichloroacetate

: 881011-62-7
(2R,3R)-2-Hydroxy-3-(4-methoxy-phenyl)-3-(2-nitro-phenylsulfanyl)-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: t-BuOK / tetrahydrofuran / -40 °C

2: toluene / 20 °C

3: glucose; MgSO₄; CaCO₃ / bakers' yeast / aq. phosphate buffer / 144 h / 35 °C

With D-glucose; potassium tert-butylate; magnesium sulfate; calcium carbonate; bakers' yeast; In tetrahydrofuran; phosphate buffer; toluene; 1: Darzens condensation;
DOI:10.3987/COM-05-S(K)57