Technology Process of 2'-O--9-β-D-xylofuranosyladenine
There total 3 articles about 2'-O--9-β-D-xylofuranosyladenine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acidic Dowex 50 WX2;
In
ethanol; water;
for 1h;
Ambient temperature;
DOI:10.1021/jm00356a010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine, dicyclohexylcarbodiimide / 96 h / Ambient temperature
2: 37 percent / acidic Dowex 50 WX2 / ethanol; H2O / 1 h / Ambient temperature
With
pyridine; acidic Dowex 50 WX2; dicyclohexyl-carbodiimide;
In
ethanol; water;
DOI:10.1021/jm00356a010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 52 percent / triethyl orthoformate, 6 M HCl / dimethylformamide / 168 h / Ambient temperature
2: pyridine, dicyclohexylcarbodiimide / 96 h / Ambient temperature
3: 37 percent / acidic Dowex 50 WX2 / ethanol; H2O / 1 h / Ambient temperature
With
pyridine; hydrogenchloride; acidic Dowex 50 WX2; orthoformic acid triethyl ester; dicyclohexyl-carbodiimide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00356a010
