2'-O--9-β-D-xylofuranosyladenine

Base Information

Chemical Name:2'-O--9-β-D-xylofuranosyladenine
CAS No.:83649-43-8
Molecular Formula:C₂₇H₂₈N₆O₇
Molecular Weight:548.555
Hs Code.:

2'-O-<N-(benzyloxycarbonyl)-L-phenylalanyl>-9-β-D-xylofuranosyladenine

Synonyms:2'-O--9-β-D-xylofuranosyladenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-O--9-β-D-xylofuranosyladenine

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Technology Process of 2'-O--9-β-D-xylofuranosyladenine

There total 3 articles about 2'-O--9-β-D-xylofuranosyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 83649-49-4
9-<2-O--3,5-O-isopropylidene-β-D-xylofuranosyl>adenine

: 83649-43-8
2'-O--9-β-D-xylofuranosyladenine

Guidance literature:: With acidic Dowex 50 WX₂; In ethanol; water; for 1h; Ambient temperature;
DOI:10.1021/jm00356a010

Reference yield:

: 7687-49-2
9-(3,5-O-isopropylidene-β-D-xylofuranosyl)adenine

: 83649-43-8
2'-O--9-β-D-xylofuranosyladenine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, dicyclohexylcarbodiimide / 96 h / Ambient temperature

2: 37 percent / acidic Dowex 50 WX₂ / ethanol; H₂O / 1 h / Ambient temperature

With pyridine; acidic Dowex 50 WX₂; dicyclohexyl-carbodiimide; In ethanol; water;
DOI:10.1021/jm00356a010

Reference yield:

: 524-69-6
adenine xyloside

: 83649-43-8
2'-O--9-β-D-xylofuranosyladenine

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / triethyl orthoformate, 6 M HCl / dimethylformamide / 168 h / Ambient temperature

2: pyridine, dicyclohexylcarbodiimide / 96 h / Ambient temperature

3: 37 percent / acidic Dowex 50 WX₂ / ethanol; H₂O / 1 h / Ambient temperature

With pyridine; hydrogenchloride; acidic Dowex 50 WX₂; orthoformic acid triethyl ester; dicyclohexyl-carbodiimide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00356a010