N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine

Base Information

• Chemical Name: N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine
• CAS No.: 157566-75-1
• Molecular Formula: C₂₇H₃₈N₂O₅
• Molecular Weight: 470.609

Synonyms:N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine

Chemical Property of N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine

Chemical Property:

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Technology Process of N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine

There total 1 articles about N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N₁-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-1-(N-isobutylamino)-4-phenylbutane (143224-62-8) → N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N1-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine (157566-75-1)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 21h;

Reference yield:

N-[(1,1-dimethylethoxyl)carbonyl]-N-[2-methylpropyl]-3S-[N1-(penylmethoxycarbonyl)amino]-2R-hydroxy-4-phenylbutylamine (157566-75-1) → tert-butyl (2R,3S)-3-amino-2-hydroxy-4-phenylbutyl(isobutyl)carbamate (183554-00-9)

Guidance literature:

With hydrogen; 5%-palladium/activated carbon; In ethanol; under 2327.23 Torr;

upstream raw materials:

di-tert-butyl dicarbonate

(2R,3S)-3-benzyloxycarbonylamino-2-hydroxy-1-(N-isobutylamino)-4-phenylbutane

Downstream raw materials:

tert-butyl (2R,3S)-3-amino-2-hydroxy-4-phenylbutyl(isobutyl)carbamate

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