(+)-8-phenylmenthyl azidoacetate

Base Information

• Chemical Name: (+)-8-phenylmenthyl azidoacetate
• CAS No.: 130156-94-4
• Molecular Formula: C₁₈H₂₅N₃O₂
• Molecular Weight: 315.415

Synonyms:(+)-8-phenylmenthyl azidoacetate

Chemical Property of (+)-8-phenylmenthyl azidoacetate

Chemical Property:

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Technology Process of (+)-8-phenylmenthyl azidoacetate

There total 3 articles about (+)-8-phenylmenthyl azidoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,2S,5R)-(+)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl chloroacetate (71804-27-8) → (+)-8-phenylmenthyl azidoacetate (130156-94-4)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 25 ℃; for 16h;

DOI:10.1016/S0957-4166(00)82310-1

Reference yield:

bromoacetic acid (-)-8-phenylmenthol ester (80595-59-1) → (+)-8-phenylmenthyl azidoacetate (130156-94-4)

Guidance literature:

With tetramethylammonium azide;

DOI:10.1016/0040-4039(95)02264-3

Reference yield:

(-)-8-phenylmenthol (65253-04-5) → (+)-8-phenylmenthyl azidoacetate (130156-94-4)

Guidance literature:

Multi-step reaction with 2 steps

2: Me₄NN₃

With tetramethylammonium azide;

DOI:10.1016/0040-4039(95)02264-3

upstream raw materials:

(1R,2S,5R)-(+)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl chloroacetate

bromoacetic acid (-)-8-phenylmenthol ester

(-)-8-phenylmenthol

Downstream raw materials:

(+)-8-phenylmenthyl-formylamido acetate

(-)-8-phenylmenthan-3-yl glycinate

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