Technology Process of C37H51NO4Si
There total 4 articles about C37H51NO4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0);
In
toluene;
at 90 ℃;
for 24h;
DOI:10.1021/ja071057p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / diisopropylethylamine / CH2Cl2 / 20 °C
2: 74 percent / sodium tert-butoxide / 1,1-bis(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium / toluene / 24 h / 90 °C
3: 82 percent / sodium tert-butoxide / 1,1-bis(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium / toluene / 24 h / 90 °C
With
N-ethyl-N,N-diisopropylamine; sodium t-butanolate;
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0);
In
dichloromethane; toluene;
2: Buchwald-Hartwig reaction / 3: Buchwald-Hartwig reaction;
DOI:10.1021/ja071057p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Et3N / PdCl2(PPh3)2; CuI / tetrahydrofuran / Heating
2: 82 percent / sodium tert-butoxide / 1,1-bis(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium / toluene / 24 h / 90 °C
With
triethylamine; sodium t-butanolate;
bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide;
In
tetrahydrofuran; toluene;
1: Sonogashira coupling / 2: Buchwald-Hartwig reaction;
DOI:10.1021/ja071057p
