C₂₂H₂₃ClF₂O₆S₂

Base Information

• Chemical Name: C₂₂H₂₃ClF₂O₆S₂
• CAS No.: 1100361-41-8
• Molecular Formula: C₂₂H₂₃ClF₂O₆S₂
• Molecular Weight: 521.003
• Mol file: 1100361-41-8.mol

Synonyms:C₂₂H₂₃ClF₂O₆S₂

Chemical Property of C₂₂H₂₃ClF₂O₆S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₃ClF₂O₆S₂

There total 14 articles about C₂₂H₂₃ClF₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H23ClF2O4S2 → C22H23ClF2O6S2 (1100361-41-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

C20H19ClF2O5S (1100361-34-9) → C22H23ClF2O6S2 (1100361-41-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 20 °C

2: potassium hydroxide / ethanol / 70 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In ethanol; dichloromethane;

DOI:10.1021/ml300044f

Reference yield:

C16H13ClF2O2S → C22H23ClF2O6S2 (1100361-41-8)

Guidance literature:

Multi-step reaction with 10 steps

1.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -78 - 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / Reflux

4.1: oxone / acetone; water / 3 h / 50 °C

5.1: methanesulfonyl chloride; triethylamine / dichloromethane / 1.5 h / 20 °C

5.2: 0.5 h / 20 °C

6.1: ozone; sodium tetrahydroborate; methanol / dichloromethane / -78 - 20 °C / Inert atmosphere

6.2: 1 h / Inert atmosphere

7.1: chiralcel OJ / isopropyl alcohol; hexane / Resolution of racemate

8.1: triethylamine / dichloromethane / 20 °C

9.1: potassium hydroxide / ethanol / 70 °C

10.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With methanol; sodium tetrahydroborate; oxone; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; Dess-Martin periodane; ozone; methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In ethanol; hexane; dichloromethane; water; isopropyl alcohol; acetone;

DOI:10.1021/ml300044f

upstream raw materials:

C₂₀H₁₉ClF₂O₅S

C₂₇H₂₅ClF₂O₇S₂

2-[(4-chloro-phenylsulfanyl)-(2,3,6-trifluoro-phenyl)-methyl]-propane-1,3-diol

2-(2,3,6-trifluoro-benzylidene)-malonic acid dimethyl ester