C₂₂H₂₃ClF₂O₆S₂

Base Information

Chemical Name:C₂₂H₂₃ClF₂O₆S₂
CAS No.:1100361-41-8
Molecular Formula:C₂₂H₂₃ClF₂O₆S₂
Molecular Weight:521.003
Hs Code.:

C<sub>22</sub>H<sub>23</sub>ClF<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₂₂H₂₃ClF₂O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₃ClF₂O₆S₂

Chemical Property:

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Technology Process of C₂₂H₂₃ClF₂O₆S₂

There total 14 articles about C₂₂H₂₃ClF₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₃ClF₂O₄S₂

: 1100361-41-8
C₂₂H₂₃ClF₂O₆S₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1100361-34-9
C₂₀H₁₉ClF₂O₅S

: 1100361-41-8
C₂₂H₂₃ClF₂O₆S₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 20 °C

2: potassium hydroxide / ethanol / 70 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In ethanol; dichloromethane;
DOI:10.1021/ml300044f

Reference yield:

: C₁₆H₁₃ClF₂O₂S

: 1100361-41-8
C₂₂H₂₃ClF₂O₆S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -78 - 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / Reflux

4.1: oxone / acetone; water / 3 h / 50 °C

5.1: methanesulfonyl chloride; triethylamine / dichloromethane / 1.5 h / 20 °C

5.2: 0.5 h / 20 °C

6.1: ozone; sodium tetrahydroborate; methanol / dichloromethane / -78 - 20 °C / Inert atmosphere

6.2: 1 h / Inert atmosphere

7.1: chiralcel OJ / isopropyl alcohol; hexane / Resolution of racemate

8.1: triethylamine / dichloromethane / 20 °C

9.1: potassium hydroxide / ethanol / 70 °C

10.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With methanol; sodium tetrahydroborate; oxone; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; Dess-Martin periodane; ozone; methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In ethanol; hexane; dichloromethane; water; isopropyl alcohol; acetone;
DOI:10.1021/ml300044f