Technology Process of C42H70O5Si2
There total 11 articles about C42H70O5Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
20 % Pd(OH)2/C; hydrogen;
In
methanol; ethyl acetate;
at 20 ℃;
for 72h;
DOI:10.1021/ol902778y
- Guidance literature:
-
With
10% palladium on activated charcoal; hydrogen;
In
ethyl acetate;
at 20 ℃;
DOI:10.1002/chem.201003135
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C
1.2: 20 °C
2.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C
3.1: 2,6-dimethylpyridine / dichloromethane / 0 °C
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer
5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C
6.1: potassium tert-butylate / tetrahydrofuran / 0 °C
7.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -60 - -25 °C
8.1: 10% palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C
With
2,6-dimethylpyridine; triethylsilane; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; magnesium bromide diethyl etherate; 10% palladium on activated charcoal; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1002/chem.201003135