(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

Base Information

Chemical Name:(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol
CAS No.:1417654-58-0
Molecular Formula:C₁₇H₁₉I₂NO₃
Molecular Weight:539.152
Hs Code.:

Synonyms:(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

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Chemical Property of (S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

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Technology Process of (S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

There total 4 articles about (S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1417654-56-8
(S)-2-((tert-butoxycarbonyl)amino)-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propanoic acid

: 1417654-58-0
(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

Guidance literature:: With lithium borohydride; chloro-trimethyl-silane; In tetrahydrofuran; 1,4-dioxane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 128781-80-6
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-(4-hydroxy-3,5-diiodophenyl)propanoate

: 1417654-58-0
(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: copper diacetate; triethylamine / dichloromethane / Molecular sieve

2: lithium hydroxide / tetrahydrofuran / 2 h

3: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran; 1,4-dioxane / 0 - 20 °C / Inert atmosphere

With lithium borohydride; chloro-trimethyl-silane; copper diacetate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1417654-55-7
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propanoate

: 1417654-58-0
(S)-2-amino-3-(3,5-diiodo-4-(4-methoxy-3-methylphenoxy)phenyl)propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran / 2 h

2: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran; 1,4-dioxane / 0 - 20 °C / Inert atmosphere

With lithium borohydride; chloro-trimethyl-silane; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane;