N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide

Base Information

• Chemical Name: N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide
• CAS No.: 365530-90-1
• Molecular Formula: C₃₈H₃₇N₃O₅
• Molecular Weight: 615.729

Synonyms:N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide

Chemical Property of N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide

Chemical Property:

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Technology Process of N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide

There total 2 articles about N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + X=(N-(E)-4-Ph-N=N-C6H4-CO)-D-threoninol (365530-89-8) → N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide (365530-90-1)

Guidance literature:

With pyridine; dmap; In dichloromethane;

DOI:10.1002/1521-3773(20010716)40:14<2671::AID-ANIE2671>3.0.CO;2-Z

Reference yield:

(E)-4-(phenyldiazenyl)benzoic acid (37790-20-8) → N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide (365530-90-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide

2: 63 percent / pyridine; DMAP / CH₂Cl₂

With pyridine; dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/1521-3773(20010716)40:14<2671::AID-ANIE2671>3.0.CO;2-Z

Reference yield:

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) + N-{(1S,2S)-1-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-2-hydroxy-propyl}-4-phenylazo-benzamide (365530-90-1) → Diisopropyl-phosphoramidous acid (1S,2S)-3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-methyl-2-(4-phenylazo-benzoylamino)-propyl ester 2-cyano-ethyl ester

Guidance literature:

With 1H-tetrazole; In acetonitrile;

DOI:10.1002/1521-3773(20010716)40:14<2671::AID-ANIE2671>3.0.CO;2-Z

upstream raw materials:

4,4'-dimethoxytrityl chloride

X=(N-(E)-4-Ph-N=N-C₆H₄-CO)-D-threoninol

(E)-4-(phenyldiazenyl)benzoic acid

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