Technology Process of C54H74O7S
There total 5 articles about C54H74O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: HCl / toluene
1.2: 74 percent / hexamethylphosphoric acid triamide
2.1: cysteamine; dithioerythritol / hexamethylphosphoric acid triamide
With
hydrogenchloride; 1,4-dithio-erythritol; Cysteamine;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; toluene;
DOI:10.1021/ol991211f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / CH(OMe)3
2: 84 percent / NaH; Bu4NBr / tetrahydrofuran
3: 93 percent / NBS; BaCO3 / CCl4 / Heating
4: cysteamine; dithioerythritol / hexamethylphosphoric acid triamide
With
N-Bromosuccinimide; 1,4-dithio-erythritol; tetrabutylammomium bromide; sodium hydride; Cysteamine; barium carbonate; trimethyl orthoformate;
In
tetrahydrofuran; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ol991211f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / NaH; Bu4NBr / tetrahydrofuran
2: 93 percent / NBS; BaCO3 / CCl4 / Heating
3: cysteamine; dithioerythritol / hexamethylphosphoric acid triamide
With
N-Bromosuccinimide; 1,4-dithio-erythritol; tetrabutylammomium bromide; sodium hydride; Cysteamine; barium carbonate;
In
tetrahydrofuran; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ol991211f