N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

Base Information

Chemical Name:N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine
CAS No.:1413917-19-7
Molecular Formula:C₂₃H₂₄N₂O₂Si
Molecular Weight:388.541
Hs Code.:

Synonyms:N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

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Chemical Property of N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

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Technology Process of N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

There total 1 articles about N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 119645-09-9
N-[(1,1-dimethylethyl)diphenylsilyl]benzenemethanamine

: 1413917-19-7
N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

Guidance literature:: N-[(1,1-dimethylethyl)diphenylsilyl]benzenemethanamine; With tert-butylhypochlorite; In chloroform; at 0 ℃; for 3h; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In diethyl ether; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jo302182t

Reference yield: 66.0%

: 1413917-19-7
N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

: 1413917-21-1
N-[(1,1-dimethylethyl)diphenylsilyl]-3(4-nitrophenyl)oxaziridine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo302182t

Reference yield:

: 1413917-19-7
N-[(1,1-dimethylethyl)diphenylsilyl]-4-nitrobenzaldimine

: 92043-24-8
4-nitro-benzaldehyde cyclohexylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid; potassium hydroxide / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

2: acetonitrile / 20 °C

With 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1021/jo302182t