ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate

Base Information

• Chemical Name: ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate
• CAS No.: 1025370-30-2
• Molecular Formula: C₄₄H₅₂N₄O₈
• Molecular Weight: 764.919

Synonyms:ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate

Chemical Property of ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate

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Technology Process of ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate

There total 1 articles about ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl (1R,2S)-1-({(4R)-1-[(2S)-2-({[(2,2-dimethylpent-4-en-1-yl)oxy]carbonyl}amino)non-8-enoyl]-4-[(7-methoxy-2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolyl}amino)-2-vinylcyclopropanecarboxylate (1025370-27-7) → ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxylate (1025370-30-2)

Guidance literature:

Zhan catalyst-1B; In dichloromethane; for 7.5h; Heating / reflux;

Reference yield:

ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxylate (1025370-30-2) → (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1(35),12,26,28,30,31,33,35-octaene-9-carboxylic acid (1025366-80-6)

Guidance literature:

ethyl (3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylate; With lithium hydroxide; water; In tetrahydrofuran; ethanol; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; ethanol; water;

upstream raw materials:

ethyl (1R,2S)-1-({(4R)-1-[(2S)-2-({[(2,2-dimethylpent-4-en-1-yl)oxy]carbonyl}amino)non-8-enoyl]-4-[(7-methoxy-2-phenyl-6-vinylquinolin-4-yl)oxy]-L-prolyl}amino)-2-vinylcyclopropanecarboxylate

Downstream raw materials:

(3R,6S,9R,11S,12Z,19S,26E)-29-methoxy-24,24-dimethyl-7,21,37-trioxo-33-phenyl-2,22-dioxa-5,8,20,32-tetraazahexacyclo[26.6.2.13,6.15,19.09,11.031,35]octatriaconta-1⁽³⁵⁾,12,26,28,30,31,33,35-octaene-9-carboxylic acid

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