tungsten tris(neopentyl)neopentylidyne

Base Information

Chemical Name:tungsten tris(neopentyl)neopentylidyne
CAS No.:68490-69-7
Molecular Formula:C₂₀H₄₂W
Molecular Weight:466.403
Hs Code.:

Synonyms:tungsten tris(neopentyl)neopentylidyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tungsten tris(neopentyl)neopentylidyne

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of tungsten tris(neopentyl)neopentylidyne

There total 3 articles about tungsten tris(neopentyl)neopentylidyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 7412-67-1
neopentyl lithium

: 13283-01-7
tungsten(VI) chloride

: 68490-69-7
tungsten tris(neopentyl)neopentylidyne

Guidance literature:: In diethyl ether; byproducts: LiCl; Me3CCH2Li in Et2O was added dropwise to WCl6 in Et2O (N2); stirring for15 min; filtration, evapn., extn. with hexane, filtration, distn. in vac.;
DOI:10.1021/om00072a018

Reference yield:

: 13470-14-9
tungsten(V) chloride

: 7412-67-1
neopentyl lithium

: 68490-69-7
tungsten tris(neopentyl)neopentylidyne

Guidance literature:: In diethyl ether; byproducts: LiCl; at -78°C (N2); filtration, evapn., extn. with hexane, filtration, distn. in vac.;
DOI:10.1021/om00072a018