Technology Process of Tungsten pentachloride
There total 24 articles about Tungsten pentachloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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In
neat (no solvent);
heated from 470°C to 550°C; elem. anal.;
- Guidance literature:
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In
neat (no solvent);
byproducts: PCl3; mixing of WS3 and solid PCl5 in a 1:2 or 1:1 molar ratio; heating in a sealed evacuated quartz ampoule at 180°C for 5 h; opening of the ampoule and removing of PCl3 under vac. at 80°C; heating the solid residue under vac.;; sublimation under vac.; identification by chem. and X-ray phase anal.;;
- Guidance literature:
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byproducts: chlorine; heating in CO2 for 18 h;
