benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

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Chemical Name:benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside
CAS No.:1004553-87-0
Molecular Formula:C₅₆H₆₀O₁₀
Molecular Weight:893.086
Hs Code.:

Synonyms:benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

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Chemical Property of benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

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Technology Process of benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

There total 1 articles about benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1004553-85-8
benzyl 4-O-allyl-β-L-xyloside

: 100-39-0
benzyl bromide

: 180714-32-3
2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl trichloroacetimidate

: 1004553-87-0
benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

: 1004553-86-9
benzyl 4-O-allyl-3-O-benzyl-2-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

Guidance literature:: benzyl 4-O-allyl-β-L-xyloside; 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl trichloroacetimidate; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h;

With potassium cyanide; In methanol; at 50 ℃; for 12h;

benzyl bromide; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1071/CH07188

Reference yield: 98.0%

: 1004553-87-0
benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside

: benzyl 2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xylopyranoside

Guidance literature:: benzyl 4-O-allyl-2-O-benzyl-3-O-(tetra-O-benzyl-β-D-glucopyranosyl)-β-L-xyloside; Wilkinson's catalyst; In ethanol; for 3h; Heating;

With hydrogenchloride; In ethanol; for 1h; Further stages.; Heating;
DOI:10.1071/CH07188