(E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde

Base Information

• Chemical Name: (E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde
• CAS No.: 1587691-65-3
• Molecular Formula: C₂₇H₂₇NO₃S
• Molecular Weight: 445.582
• Mol file: 1587691-65-3.mol

Synonyms:(E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde

Chemical Property of (E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of (E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde

There total 1 articles about (E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

C20H22BrNO2S (1587691-51-7) + 2-formylbenzene boronic acid (40138-16-7) → (E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde (1587691-65-3)

Guidance literature:

With palladium diacetate; potassium carbonate; tricyclohexylphosphine; In ethanol; water; toluene; at 90 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol500505k

Reference yield: 90.0%

(E)-2-(p-tolyl(1-tosylindolin-3-ylidene)methyl)benzaldehyde (1587691-65-3) → 11-butyl-5-tosyl-5H-benzo[b]carbazole (1587691-85-7)

Guidance literature:

With iron(III) chloride; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol500505k

upstream raw materials:

C₂₀H₂₂BrNO₂S

2-formylbenzene boronic acid

Downstream raw materials:

11-butyl-5-tosyl-5H-benzo[b]carbazole