2,3-dihydrospiroanthrone-3,10'-anthrone>

Base Information

• Chemical Name: 2,3-dihydrospiroanthrone-3,10'-anthrone>
• CAS No.: 65252-95-1
• Molecular Formula: C₃₀H₁₈O₂
• Molecular Weight: 410.472

Synonyms:2,3-dihydrospiroanthrone-3,10'-anthrone>

Chemical Property of 2,3-dihydrospiroanthrone-3,10'-anthrone>

Chemical Property:

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Technology Process of 2,3-dihydrospiroanthrone-3,10'-anthrone>

There total 3 articles about 2,3-dihydrospiroanthrone-3,10'-anthrone> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

10-Methylene-10H-anthracen-9-one (4159-04-0) → 10,10'-(1,2-ethanediylidene)bisanthrone (5816-02-4) + 10,10'-(1,2-ethanediyl)bisanthrone (58382-11-9) + 2,3-dihydrospiroanthrone-3,10'-anthrone> (65252-95-1) + 9,10-phenanthrenequinone (84-65-1)

Guidance literature:

at 148 ℃; for 15h; in sealed test tube;

DOI:10.1246/bcsj.59.319

Reference yield:

10-Methylene-10H-anthracen-9-one (4159-04-0) → 2,3-dihydrospiroanthrone-3,10'-anthrone> (65252-95-1) + C22H17N3O (73078-96-3) + C30H26N2O (73079-12-6)

Guidance literature:

With p-methylazidobenzene; at 90 ℃; Yield given. Yields of byproduct given;

DOI:10.1021/jo01297a028

Reference yield:

10-Methylene-10H-anthracen-9-one (4159-04-0) + Phenyl azide (622-37-7) → 10-phenylimino-9,10-dihydroanthracen-9-one (10019-06-4) + 2,3-dihydrospiroanthrone-3,10'-anthrone> (65252-95-1) + 1'-phenylspiro (73078-95-2) + 1',3'-diphenylspiro (73079-11-5)

Guidance literature:

at 90 ℃; Yield given. Yields of byproduct given;

DOI:10.1021/jo01297a028

upstream raw materials:

10-Methylene-10H-anthracen-9-one

Phenyl azide

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