trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

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Chemical Name:trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester
CAS No.:776298-22-7
Molecular Formula:C₃₃H₃₂BrF₃O₇S
Molecular Weight:709.578
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

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Chemical Property of trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

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Technology Process of trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

There total 15 articles about trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 776298-22-7
trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄ / tetrahydrofuran / 1 h / 0 - 20 °C

2: CBr₄; PPh₃ / acetonitrile / 9 h / 20 °C

3: 3 h / 90 °C

4: 75 percent / NaH / tetrahydrofuran / 3 h / 0 - 20 °C

5: H₂ / PtO₂ / CH₂Cl₂ / 6 h / 20 °C

6: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; hydrogen; sodium hydride; triethylamine; triphenylphosphine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; acetonitrile; 3: Arbuzov reaction;
DOI:10.1016/j.tetlet.2004.07.068

Reference yield:

: 19614-12-1
2-bromo-5-methoxybenzyl bromide

: 776298-22-7
trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 2 h / 90 °C

2: 73 percent / NaH / tetrahydrofuran / 0 - 20 °C

3: 75 percent / NaH / tetrahydrofuran / 3 h / 0 - 20 °C

4: H₂ / PtO₂ / CH₂Cl₂ / 6 h / 20 °C

5: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

With hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; 1: Arbuzov reaction;
DOI:10.1016/j.tetlet.2004.07.068

Reference yield:

: 4877-93-4
2,2'-Dimethoxybiphenyl

: 776298-22-7
trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / 0 - 90 °C

2: 73 percent / NaH / tetrahydrofuran / 0 - 20 °C

3: 75 percent / NaH / tetrahydrofuran / 3 h / 0 - 20 °C

4: H₂ / PtO₂ / CH₂Cl₂ / 6 h / 20 °C

5: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

With hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; trifluoroacetic acid;
DOI:10.1016/j.tetlet.2004.07.068