trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester
CAS No.:776298-34-1
Molecular Formula:C₃₉H₄₄BF₃O₉S
Molecular Weight:756.645
Hs Code.:

trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

Synonyms:trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

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Chemical Property of trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

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Technology Process of trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

There total 15 articles about trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 73183-34-3
bis(pinacol)diborane

: 776298-22-7
trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

: 776298-34-1
trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

Guidance literature:: With potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 1.5h;
DOI:10.1016/j.tetlet.2004.07.068

Reference yield: 40.0%

: 73183-34-3
bis(pinacol)diborane

: 776298-22-7
trifluoro-methanesulfonic acid 4-(2-{5'-[2-(2-bromo-5-methoxy-phenyl)-ethyl]-6,2'-dimethoxy-biphenyl-3-yl}-ethyl)-2-methoxy-phenyl ester

: 776298-34-1
trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

: C₄₄H₅₆B₂O₈

Guidance literature:: With potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1016/j.tetlet.2004.07.068

Reference yield:

: 33693-48-0
4-benzyloxy-3-methoxybenzyl alcohol

: 776298-34-1
trifluoro-methanesulfonic acid 4-[2-(6,2'-dimethoxy-5'-{2-[5-methoxy-2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-biphenyl-3-yl)-ethyl]-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: CBr₄; PPh₃ / acetonitrile / 9 h / 20 °C

2: 3 h / 90 °C

3: 75 percent / NaH / tetrahydrofuran / 3 h / 0 - 20 °C

4: H₂ / PtO₂ / CH₂Cl₂ / 6 h / 20 °C

5: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

6: 63 percent / AcOK / dimethylformamide / 1.5 h / 80 °C

With carbon tetrabromide; hydrogen; potassium acetate; sodium hydride; triethylamine; triphenylphosphine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: Arbuzov reaction;
DOI:10.1016/j.tetlet.2004.07.068