<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

Base Information

Chemical Name:<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile
CAS No.:147362-14-9
Molecular Formula:C₁₉H₁₆N₄O₃S
Molecular Weight:380.427
Hs Code.:

Synonyms:<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

Suppliers and Price of <1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

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Technology Process of <1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

There total 4 articles about <1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 98-59-9
p-toluenesulfonyl chloride

: 147344-76-1
<1-(2-hydroxyethyl)-2-benzimidazolidinylidene>propanedinitrile

: 147362-14-9
<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

Guidance literature:: With pyridine; for 8h; Ambient temperature;
DOI:10.1021/jm00057a007

Reference yield:

: 4926-55-0
2-[(2-nitrophenyl)amino]ethanol

: 147362-14-9
<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / H₂ / 10percent Pd/C / ethanol / 0.5 h / Ambient temperature

2: 77 percent / 0.25 h / 80 °C

3: 76 percent / pyridine / 8 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00057a007

Reference yield:

: 577-19-5
2-nitrophenyl bromide

: 147362-14-9
<1-<2-<(p-tolylsulfonyl)oxy>ethyl>-2-benzimidazolidinylidene>propanedinitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / 8 h / 100 °C

2: 97 percent / H₂ / 10percent Pd/C / ethanol / 0.5 h / Ambient temperature

3: 77 percent / 0.25 h / 80 °C

4: 76 percent / pyridine / 8 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00057a007