(E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal

Base Information

• Chemical Name: (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal
• CAS No.: 104995-51-9
• Molecular Formula: C₃₂H₃₆O₅S
• Molecular Weight: 532.701

Synonyms:(E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal

Chemical Property of (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal

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Technology Process of (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal

There total 4 articles about (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one (104995-49-5) → (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal (104995-51-9)

Guidance literature:

With manganese(IV) oxide;

DOI:10.1021/jo00374a050

Reference yield:

(E)-3-(6-Formyl-6-methyl-cyclohex-2-enyl)-but-2-enoic acid methyl ester (98993-13-6,99094-70-9,111138-05-7) → (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal (104995-51-9)

Guidance literature:

Multi-step reaction with 3 steps

3: 95 percent / MnO₂

With manganese(IV) oxide;

DOI:10.1021/jo00374a050

Reference yield:

(1R,2R)-1-Methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbaldehyde (104995-47-3) → (E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal (104995-51-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 95 percent / MnO₂

With manganese(IV) oxide;

DOI:10.1021/jo00374a050

upstream raw materials:

(5R,10R)-10-((E)-3-Hydroxy-2-methyl-propenyl)-4-methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-1-oxa-spiro[4.5]deca-3,7-dien-2-one

(E)-3-(6-Formyl-6-methyl-cyclohex-2-enyl)-but-2-enoic acid methyl ester

(1R,2R)-1-Methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbaldehyde

(5S,10S)-10-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-propenyl]-4-methoxy-1-oxa-spiro[4.5]deca-3,7-dien-2-one

Downstream raw materials:

(E)-3-{(5R,6R)-4-Methoxy-3-[(1R,2R)-1-methyl-2-((E)-1-methyl-3-phenylsulfanyl-propenyl)-cyclohex-3-enecarbonyl]-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-acrylic acid methyl ester

(E)-3-{(5R,6R)-3-[(1R,2R)-2-((E)-3-Benzenesulfonyl-1-methyl-propenyl)-1-methyl-cyclohex-3-enecarbonyl]-4-methoxy-2-oxo-1-oxa-spiro[4.5]deca-3,8-dien-6-yl}-2-methyl-propenal

C₃₂H₃₄O₇S

C₃₂H₃₆O₇S

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