C₄₁H₃₉BF₂N₂O₂

Base Information

Chemical Name:C₄₁H₃₉BF₂N₂O₂
CAS No.:1303477-77-1
Molecular Formula:C₄₁H₃₉BF₂N₂O₂
Molecular Weight:640.581
Hs Code.:

C<sub>41</sub>H<sub>39</sub>BF<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₄₁H₃₉BF₂N₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₃₉BF₂N₂O₂

Chemical Property:

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Technology Process of C₄₁H₃₉BF₂N₂O₂

There total 3 articles about C₄₁H₃₉BF₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1303477-74-8
C₁₇H₁₉NO

: 100-52-7
benzaldehyde

: 1303477-77-1
C₄₁H₃₉BF₂N₂O₂

Guidance literature:: C₁₇H₁₉NO; benzaldehyde; With trifluoroacetic acid; In dichloromethane; for 18h; Reflux; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.016

Reference yield:

: 5720-06-9
2-Methoxyphenylboronic acid

: 1303477-77-1
C₄₁H₃₉BF₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 5 h / Reflux; Inert atmosphere

2.1: potassium hydroxide / ethylene glycol / 2 h / 160 °C / Inert atmosphere; Darkness

3.1: trifluoroacetic acid / dichloromethane / 18 h / Reflux; Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

3.3: 0.5 h / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; potassium hydroxide; In dichloromethane; ethylene glycol; N,N-dimethyl-formamide; 1.1: Suzuki coupling;
DOI:10.1016/j.tet.2011.03.016

Reference yield:

: ethyl 3-iodo-4,5,6,7-tetrahydro-4,7-ethano-2H-isoindole-1-carboxylate

: 1303477-77-1
C₄₁H₃₉BF₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / N,N-dimethyl-formamide / 5 h / Reflux; Inert atmosphere

2.1: potassium hydroxide / ethylene glycol / 2 h / 160 °C / Inert atmosphere; Darkness

3.1: trifluoroacetic acid / dichloromethane / 18 h / Reflux; Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

3.3: 0.5 h / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; potassium hydroxide; In dichloromethane; ethylene glycol; N,N-dimethyl-formamide; 1.1: Suzuki coupling;
DOI:10.1016/j.tet.2011.03.016