8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

Base Information

Chemical Name:8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine
CAS No.:403821-75-0
Molecular Formula:C₁₂H₁₁ClN₈S
Molecular Weight:334.792
Hs Code.:

8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-<i>a</i>][1,3,5]triazine-2,7-diamine

Synonyms:8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

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Chemical Property of 8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

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Technology Process of 8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

There total 3 articles about 8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 10191-60-3
dimethyl N-cyanodithioiminocarbonate

: 3656-04-0
3,5-diamino-4-(p-chlorophenylazo)pyrazole

: 403821-75-0
8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

Guidance literature:: With piperidine; for 3h; Heating;

Reference yield:

: 2,7-diamino-8-(4-chlorophenyldiazenyl)pyrazolo[1,5-a][1,3,5]triazine-4-thiol

: 74-88-4
methyl iodide

: 403821-75-0
8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

Guidance literature:: 2,7-diamino-8-(4-chlorophenyldiazenyl)pyrazolo[1,5-a][1,3,5]triazine-4-thiol; With sodium ethanolate; for 0.5h; Reflux;

methyl iodide; for 3h; Reflux;
DOI:10.1080/15257770.2015.1078470

Reference yield:

: 3656-04-0
3,5-diamino-4-(p-chlorophenylazo)pyrazole

: 403821-75-0
8-(4-chloro-phenylazo)-4-methylsulfanyl-pyrazolo[1,5-a][1,3,5]triazine-2,7-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 0.17 h / 150 °C / Microwave irradiation

2.1: sodium ethanolate / 0.5 h / Reflux

2.2: 3 h / Reflux

With sodium ethanolate; acetic acid;
DOI:10.1080/15257770.2015.1078470