C₁₆H₂₁NO₃

Base Information

Chemical Name:C₁₆H₂₁NO₃
CAS No.:1271773-31-9
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

C<sub>16</sub>H<sub>21</sub>NO<sub>3</sub>

Synonyms:C₁₆H₂₁NO₃

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Chemical Property of C₁₆H₂₁NO₃

Chemical Property:

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Technology Process of C₁₆H₂₁NO₃

There total 7 articles about C₁₆H₂₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271773-27-3
C₁₆H₂₃NO₃

: 1271773-31-9
C₁₆H₂₁NO₃

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; Molecular sieves 3?;

Reference yield:

: 1271773-08-0
C₂₁H₂₁NO₃

: 1271773-31-9
C₁₆H₂₁NO₃

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

3: hydrazine hydrate / ethanol / 3 h / Heating; Reflux

4: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h

5: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C

6: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

7: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

With sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; sodium hydrogencarbonate; hydrazine hydrate; 4-methylmorpholine N-oxide; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: (S)-2-allyl-3-phenylpropan-1-ol

: 1271773-31-9
C₁₆H₂₁NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

2: hydrazine hydrate / ethanol / 3 h / Heating; Reflux

3: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h

4: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C

5: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

6: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

With sodium periodate; osmium(VIII) oxide; sodium hydrogencarbonate; hydrazine hydrate; 4-methylmorpholine N-oxide; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; tert-butyl alcohol;