C₃₆H₄₅FN₂O₆

Base Information

Chemical Name:C₃₆H₄₅FN₂O₆
CAS No.:1335557-67-9
Molecular Formula:C₃₆H₄₅FN₂O₆
Molecular Weight:620.762
Hs Code.:

C<sub>36</sub>H<sub>45</sub>FN<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₆H₄₅FN₂O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₄₅FN₂O₆

Chemical Property:

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Technology Process of C₃₆H₄₅FN₂O₆

There total 10 articles about C₃₆H₄₅FN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335557-66-8
C₃₃H₄₁FN₂O₆

: 106-95-6
allyl bromide

: 1335557-67-9
C₃₆H₄₅FN₂O₆

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; In acetonitrile; at 70 ℃; for 24h;

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 1335557-67-9
C₃₆H₄₅FN₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 12 h / 25 °C

2.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

3.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

4.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

5.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

7.2: 0.5 h / -78 °C

7.3: -78 - 20 °C

8.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

9.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; tetrabutylammomium bromide; water; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-67-9
C₃₆H₄₅FN₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

5.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

6.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

8.2: 0.5 h / -78 °C

8.3: -78 - 20 °C

9.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; sec.-butyllithium; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; In tetrahydrofuran; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile;