5-chloro-2,4-dimethoxythiophenol

Base Information

Chemical Name:5-chloro-2,4-dimethoxythiophenol
CAS No.:18858-09-8
Molecular Formula:C₈H₉ClO₂S
Molecular Weight:204.677
Hs Code.:

Synonyms:5-chloro-2,4-dimethoxythiophenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-chloro-2,4-dimethoxythiophenol

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Technology Process of 5-chloro-2,4-dimethoxythiophenol

There total 3 articles about 5-chloro-2,4-dimethoxythiophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 78046-28-3
5-chloro-2,4-dimethoxy-benzenesulfonyl chloride

: 18858-09-8
5-chloro-2,4-dimethoxythiophenol

Guidance literature:: With hydrogenchloride; zinc; In benzene; at 50 ℃; for 0.5h;
DOI:10.1039/P19810000718

Reference yield:

: 7051-13-0
1-chloro-2,4-dimethoxybenzene

: 18858-09-8
5-chloro-2,4-dimethoxythiophenol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / chlorosulphonic acid / ice bath

2: 71 percent / zinc dust, 37percent HCl / benzene / 0.5 h / 50 °C

With hydrogenchloride; chlorosulfonic acid; zinc; In benzene;
DOI:10.1039/P19810000718