methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

Base Information

Chemical Name:methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate
CAS No.:1354904-68-9
Molecular Formula:C₂₀H₁₉BrN₄O₄
Molecular Weight:459.299
Hs Code.:

Synonyms:methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

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Chemical Property of methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

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Technology Process of methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

There total 5 articles about methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 274-47-5
imidazo[1,5-a]pyridine

: 1354904-68-9
methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 1,2-dichloro-ethane / 4.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 - 80 °C / Inert atmosphere

2.1: N-Bromosuccinimide / dichloromethane / 2.5 h / Inert atmosphere

3.1: 1,4-dioxane / 1.5 h / 20 - 100 °C / Inert atmosphere

3.2: 2.5 h / 20 °C

With N-Bromosuccinimide; triethylamine; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 107-10-8,42939-71-9
propylamine

: 32315-10-9
bis(trichloromethyl) carbonate

: 944445-97-0
methyl 2-amino-5-[1-bromo-(imidazo[1,5-a]pyridine-3-yl carbonyl)]benzoate

: 1354904-68-9
methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

Guidance literature:: bis(trichloromethyl) carbonate; methyl 2-amino-5-[1-bromo-(imidazo[1,5-a]pyridine-3-yl carbonyl)]benzoate; In 1,4-dioxane; at 20 - 100 ℃; for 1.5h; Inert atmosphere;

propylamine; With triethylamine; In 1,4-dioxane; at 20 ℃; for 2.5h;

Reference yield:

: 944445-57-2
4-oxo-2-phenyl-4H-3,1-benzoxazine-6-carbonyl chloride

: 1354904-68-9
methyl 5-[(1-bromoimidazo(1,5-a)pyridin-3-yl)carbonyl]-2-(propylcarbamoyl)aminobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 1,2-dichloro-ethane / 4.5 h / 0 - 20 °C / Inert atmosphere

1.2: 20 - 80 °C / Inert atmosphere

2.1: N-Bromosuccinimide / dichloromethane / 2.5 h / Inert atmosphere

3.1: 1,4-dioxane / 1.5 h / 20 - 100 °C / Inert atmosphere

3.2: 2.5 h / 20 °C

With N-Bromosuccinimide; triethylamine; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;