methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

Base Information

Chemical Name:methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate
CAS No.:88453-67-2
Molecular Formula:C₃₁H₃₂O₇
Molecular Weight:516.591
Hs Code.:

Synonyms:methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

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Chemical Property of methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

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Technology Process of methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

There total 3 articles about methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 88453-65-0
methyl 2-<3-(3-(benzyloxy)pent-1-yl)-4-hydroxy-5-methoxyanthraquinon-2-yl>acetate

: 77-78-1
dimethyl sulfate

: 88453-67-2
methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

Guidance literature:: With potassium carbonate; triethylamine; 1.) acetone, reflux, 8 h, 2.) ethyl acetate, r.t., 0.5 h;
DOI:10.1021/ja00316a048

Reference yield:

: 88453-64-9
[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid methyl ester

: 88453-67-2
methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / dimethylformamide / 5 h / 70 °C

2: 91 percent / 1.) potassium carbonate, 2.) triethylamine / 1.) acetone, reflux, 8 h, 2.) ethyl acetate, r.t., 0.5 h

With potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00316a048

Reference yield:

: 88453-87-6
[3-(3-Benzyloxy-pentyl)-9,10-dihydroxy-5-methoxy-4-oxo-1,2,3,4-tetrahydro-anthracen-2-yl]-acetic acid tert-butyl ester

: 88453-67-2
methyl <3-(3-(benzyloxy)pent-1-yl)-4,5-dimethoxyanthraquinon-2-yl>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen chloride / methanol / 1 h / 50 °C

2: 80 percent / dimethylformamide / 5 h / 70 °C

3: 91 percent / 1.) potassium carbonate, 2.) triethylamine / 1.) acetone, reflux, 8 h, 2.) ethyl acetate, r.t., 0.5 h

With hydrogenchloride; potassium carbonate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00316a048