C₅₇H₇₅BrO₅

Base Information

• Chemical Name: C₅₇H₇₅BrO₅
• CAS No.: 1237132-99-8
• Molecular Formula: C₅₇H₇₅BrO₅
• Molecular Weight: 920.123
• Mol file: 1237132-99-8.mol

Synonyms:C₅₇H₇₅BrO₅

Chemical Property of C₅₇H₇₅BrO₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₇H₇₅BrO₅

There total 6 articles about C₅₇H₇₅BrO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C57H76O6 (1237132-97-6) → C57H75BrO5 (1237132-99-8)

Guidance literature:

With phosphorus tribromide; In toluene; at 0 - 20 ℃; for 4h;

DOI:10.1002/ejic.200901141

Reference yield:

C11H15IO2 (1237132-95-4) → C57H75BrO5 (1237132-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

2: phosphorus tribromide / toluene / 4 h / 0 - 20 °C

With phosphorus tribromide; potassium carbonate; In N,N-dimethyl-formamide; toluene;

DOI:10.1002/ejic.200901141

Reference yield:

(4-hydroxyphenyl)methanol (623-05-2) → C57H75BrO5 (1237132-99-8)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: sodium iodide / butanone / 24 h / 80 °C

3: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

4: phosphorus tribromide / toluene / 4 h / 0 - 20 °C

With phosphorus tribromide; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; toluene; butanone;

DOI:10.1002/ejic.200901141

upstream raw materials:

C₅₇H₇₆O₆

[4-(4-chlorobutoxy)phenyl]methanol

C₁₁H₁₅IO₂

C₄₆H₆₂O₄

Downstream raw materials:

(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(C(CH₃)3C₆H₄OC₃H₆)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br