1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

Base Information

Chemical Name:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine
CAS No.:136632-01-4
Molecular Formula:C₂₀H₃₀N₂O₃SSeSi
Molecular Weight:485.581
Hs Code.:

Synonyms:1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

Suppliers and Price of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

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Technology Process of 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

There total 3 articles about 1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132885-30-4
1-<(2-hydroxyethoxy)methyl>-2-thiothymine

: 136632-01-4
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / imidazole / dimethylformamide / Ambient temperature

2: 1.) LDA / 1.) THF, from -78 deg C to -70 deg C, 1 h, 2.) THF, -78 deg C, 30 min

With 1H-imidazole; lithium diisopropyl amide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00115a022

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 136632-01-4
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / imidazole / dimethylformamide / Ambient temperature

2: 1.) LDA / 1.) THF, from -78 deg C to -70 deg C, 1 h, 2.) THF, -78 deg C, 30 min

With 1H-imidazole; lithium diisopropyl amide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00115a022

Reference yield:

: 1666-13-3
diphenyl diselenide

: 132885-32-6
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-2-thiothymine

: 136632-01-4
1-<<2-<(tert-butyldimethylsilyl)oxy>ethoxy>methyl>-6-(phenylselenenyl)-2-thiothymine

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, from -78 deg C to -70 deg C, 1 h, 2.) THF, -78 deg C, 30 min;
DOI:10.1021/jm00115a022