Technology Process of C33H42O9S4
There total 1 articles about C33H42O9S4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
for 1h;
Cooling with ice;
DOI:10.1002/ejoc.201201184
- Guidance literature:
-
Multi-step reaction with 4 steps
1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 0.5 h / Cooling with ice
2: zinc; sodium iodide / N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere
3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 4 h / Inert atmosphere; Heating; Reflux
4: hydrogen; palladium 10% on activated carbon / ethanol / 48 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; sodium iodide; nickel dichloride; zinc;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
3: |Cross Metathesis;
DOI:10.1002/ejoc.201201184
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nickel dichloride; sodium tetrahydroborate / methanol; tetrahydrofuran / 0.5 h / Cooling with ice
2: zinc; sodium iodide / N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere
With
sodium tetrahydroborate; sodium iodide; nickel dichloride; zinc;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201184
