Technology Process of C22H19F6NO7S2
There total 8 articles about C22H19F6NO7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 50 °C / Inert atmosphere
2: hydrogen bromide; acetic acid / 12 h / Reflux
3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
With
hydrogen bromide; sodium hydride; acetic acid; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / acetone / 18 h / Reflux
2: phosphorus tribromide / toluene / 6 h / 0 °C / Inert atmosphere; Reflux
3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 50 °C / Inert atmosphere
4: hydrogen bromide; acetic acid / 12 h / Reflux
5: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
With
hydrogen bromide; phosphorus tribromide; sodium hydride; potassium carbonate; acetic acid; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide; acetone; toluene; mineral oil;