8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

Base Information

Chemical Name:8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one
CAS No.:123834-75-3
Molecular Formula:C₂₆H₃₄O₅
Molecular Weight:426.553
Hs Code.:

Synonyms:8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

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Technology Process of 8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

There total 7 articles about 8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 123834-74-2
7α-hydroxy-8β-(hydroxymethyl)-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

: 98-88-4
benzoyl chloride

: 123834-75-3
8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

Guidance literature:: With dmap; In pyridine; at 25 ℃; for 18h;
DOI:10.1021/jo00289a023

Reference yield:

: 54125-02-9
danishefsky's diene

: 123834-75-3
8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

Guidance literature:: Multi-step reaction with 2 steps

2: 97 percent / 4-(N,N-dimethylamino)pyridine / pyridine / 18 h / 25 °C

With dmap; In pyridine;
DOI:10.1021/jo00289a023

Reference yield:

: 100348-93-4
(R)-Wieland-Miescher ketone

: 123834-75-3
8β-((benzoyloxy)methyl)-7α-hydroxy-1β-methoxy-13-methyl-19-nor-9β-podocarp-13-en-12-one

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / NaBH₄

2: 1) NaH

6: 97 percent / 4-(N,N-dimethylamino)pyridine / pyridine / 18 h / 25 °C

With dmap; sodium tetrahydroborate; sodium hydride; In pyridine;
DOI:10.1021/jo00289a023