P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Base Information

Chemical Name:P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate
CAS No.:121192-45-8
Molecular Formula:CF₃O₃S*C₂₄H₂₆O₃P
Molecular Weight:543.505
Hs Code.:

P-<erythro-(Carbethoxy-1-deuterio-2-hydroxy-2-phenylethyl)>-P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Synonyms:P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

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Chemical Property of P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

There total 4 articles about P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 121192-45-8
P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, -78 deg C, 15 min; 2.) 15 min

2: hexane; diethyl ether; CH₂Cl₂

With n-butyllithium; diisopropylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00197a055

Reference yield:

: 121192-42-5
Ethyl (diphenylphosphino)acetate-d2

: 121192-45-8
P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, -78 deg C, 15 min; 2.) 15 min

2: hexane; diethyl ether; CH₂Cl₂

With n-butyllithium; diisopropylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00197a055

Reference yield:

: 55552-24-4
ethyl (diphenylphosphino)acetate

: 121192-45-8
P--P,P-diphenyl-P-methylphosphonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: D₂O, DBU / tetrahydrofuran / 9 h / Ambient temperature

2: 1.) n-BuLi, diisopropylamine / 1.) THF, hexane, -78 deg C, 15 min; 2.) 15 min

3: hexane; diethyl ether; CH₂Cl₂

With n-butyllithium; water-d2; 1,8-diazabicyclo[5.4.0]undec-7-ene; diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00197a055