N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

Base Information

Chemical Name:N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine
CAS No.:123150-53-8
Molecular Formula:C₂₄H₂₁NO₄
Molecular Weight:387.435
Hs Code.:

N-(benz<f>inden-3-ylmethyloxycarbonyl)phenylalanine

Synonyms:N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

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Chemical Property of N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

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Technology Process of N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

There total 6 articles about N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 150-30-1,25191-15-5,658-69-5,67675-33-6
Phenylalanine

: 123150-52-7
benzinden-3-ylmethyl azidoformate

: 123150-53-8
N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 96h;
DOI:10.1021/jo00288a042

Reference yield:

: 95-13-6
1-indene

: 123150-53-8
N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

Guidance literature:: Multi-step reaction with 4 steps

1: 5 percent / 1. n-butyl lithium 2. b) HCl / 3. Et₃N / 1. ether, THF, -70 deg C, 2 h 45 min 2. a) -50 deg C b) room temp., 15 min 3. EtOH

2: 61 percent / tetrahydrofuran / 3.5 h / 0 °C

3: 81 percent / NaN₃ / H₂O / 1. 0 deg C (ice bath), 2 h 2. room temp., 2 h

4: 76 percent / tetrahydrofuran; various solvent(s) / 96 h / 0 °C

With hydrogenchloride; n-butyllithium; sodium azide; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/jo00288a042

Reference yield:

: 268-40-6
benz [f]indene

: 123150-53-8
N-(benzinden-3-ylmethyloxycarbonyl)phenylalanine

Guidance literature:: Multi-step reaction with 5 steps

1: 1. n-butyl lithium 2. b) HCl / 1. ether, THF, -70 deg C, 2 h 45 min 2. a) -50 deg C b) room temp., 15 min

2: triethylamine, pyridine / 21 h / Ambient temperature

3: 61 percent / tetrahydrofuran / 3.5 h / 0 °C

4: 81 percent / NaN₃ / H₂O / 1. 0 deg C (ice bath), 2 h 2. room temp., 2 h

5: 76 percent / tetrahydrofuran; various solvent(s) / 96 h / 0 °C

With pyridine; hydrogenchloride; n-butyllithium; sodium azide; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/jo00288a042