{{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester

Base Information

• Chemical Name: {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester
• CAS No.: 202914-64-5
• Molecular Formula: C₃₄H₃₅N₃O₇
• Molecular Weight: 597.668

Synonyms:{{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester

Chemical Property of {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester

Chemical Property:

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Technology Process of {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester

There total 1 articles about {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

allyl alcohol (107-18-6) + {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid → {{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester (202914-64-5)

Guidance literature:

With pyridine; 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; at 0 ℃; for 24h;

DOI:10.1002/anie.199728091

Reference yield:

{{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester (202914-64-5) → C49H53N8O14P

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / 80percent HOAc / 3 h / Ambient temperature

2: 65 percent / pyridine, 3-nitro-1-(p-toluenesulfonyl)-1H-1,2,4-triazole / 14 h / 0 °C

3: 70 percent / PPh₃, diethylammonium hydrogen carbonate / Pd(PPh₃)4 / CH₂Cl₂ / 1 h

With pyridine; diethylammonium hydrogencarbonate; 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; acetic acid; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane;

DOI:10.1002/anie.199728091

Reference yield:

{{2-[(4-Methoxy-phenyl)-diphenyl-methoxy]-ethyl}-[2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-acetyl]-amino}-acetic acid allyl ester (202914-64-5) → C52H57N8O14P (202914-66-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / 80percent HOAc / 3 h / Ambient temperature

2: 65 percent / pyridine, 3-nitro-1-(p-toluenesulfonyl)-1H-1,2,4-triazole / 14 h / 0 °C

With pyridine; 1-(toluene-p-sulphonyl)-3-nitro-1,2,4-triazole; acetic acid;

DOI:10.1002/anie.199728091

upstream raw materials:

allyl alcohol

Downstream raw materials:

C₅₂H₅₇N₈O₁₄P

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