6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate

Base Information

• Chemical Name: 6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate
• CAS No.: 1202173-91-8
• Molecular Formula: C₁₁H₁₉F₃O₃SSi
• Molecular Weight: 316.417

Synonyms:6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate

Chemical Property of 6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate

Chemical Property:

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Technology Process of 6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate

There total 1 articles about 6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + 2-methyl-2-(trimethylsilyl)cyclohexanone (1202173-90-7) → 6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate (1202173-91-8)

Guidance literature:

2-methyl-2-(trimethylsilyl)cyclohexanone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.666667h; Inert atmosphere;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.200900631

Reference yield: 38.0%

6-methyl-6-(trimethylsilyl)-1-cyclohexenyl 1-trifluoromethanesulfonate (1202173-91-8) + 1,3-diphenylisobenzofuran (5471-63-6) → endo-9a-methyl-9,10-diphenyl-1,2,3,9,9a,10-hexahydro-9,10-epoxyanthracene + exo-9a-methyl-9,10-diphenyl-1,2,3,9,9a,10-hexahydro-9,10-epoxyanthracene + endo-4-methyl-9,10-diphenyl-1,2,3,9,9a,10-hexahydro-9,10-epoxyanthracene

Guidance literature:

With cesium fluoride; In tetrahydrofuran; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/ejoc.200900631

upstream raw materials:

N,N-phenylbistrifluoromethane-sulfonimide

2-methyl-2-(trimethylsilyl)cyclohexanone

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