1,4-phenylenediacetic acid-d4

Base Information

Chemical Name:1,4-phenylenediacetic acid-d4
CAS No.:104183-05-3
Molecular Formula:C₁₀H₁₀O₄
Molecular Weight:198.155
Hs Code.:

Synonyms:1,4-phenylenediacetic acid-d4

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Chemical Property of 1,4-phenylenediacetic acid-d4

Chemical Property:

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Technology Process of 1,4-phenylenediacetic acid-d4

There total 1 articles about 1,4-phenylenediacetic acid-d4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7325-46-4
1,4-phenylenediacetic acid

: 104183-05-3
1,4-phenylenediacetic acid-d4

Guidance literature:: With potassium hydroxide; diclazuril; water; water-d2; Yield given. Multistep reaction; 1.) 260 deg C, 88 h; 2.) 160 deg C, 24 h;
DOI:10.1139/v86-179

Reference yield:

: 104183-05-3
1,4-phenylenediacetic acid-d4

: C₂₅H₂₀BrO₃⁽¹⁺⁾*BF₄^(1-)

: C₅₈H₄₀⁽²⁾H₄Br₂O₄

Guidance literature:: 1,4-phenylenediacetic acid-d4; With sodium methylate; In methanol; at 20 ℃; for 0.5h;

C₂₅H₂₀BrO₃⁽¹⁺⁾*BF₄^(1-); In acetic anhydride; at 150 ℃; for 6h;
DOI:10.1039/b807382a

Reference yield:

: 64-17-5
ethanol

: 104183-05-3
1,4-phenylenediacetic acid-d4

: 104183-10-0
benzenediethanol-d4

Guidance literature:: With lithium aluminium tetrahydride; sulfuric acid; Yield given. Multistep reaction; 1.) benzene, reflux, 18 h; 2.) ether, reflux;
DOI:10.1139/v86-179