N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

Base Information

Chemical Name:N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine
CAS No.:863559-77-7
Molecular Formula:C₁₄H₂₉NO₂Si
Molecular Weight:271.475
Hs Code.:

Synonyms:N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

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Chemical Property of N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

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Technology Process of N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

There total 1 articles about N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: N-(methoxycarbonyl)-(R)-(-)-1-cyclohexylethylamine

: 4206-67-1
iodo(trimethylsilyl)methane

: 863559-77-7
N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

Guidance literature:: N-(methoxycarbonyl)-(R)-(-)-1-cyclohexylethylamine; With sodium hydride; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 4h;

iodo(trimethylsilyl)methane; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 3h;
DOI:10.1246/bcsj.78.1206

Reference yield: 46.0%

: 863559-77-7
N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

: 7642-15-1
(Z)-oct-4-ene

: 3-((R)-(-)-1-cyclohexylethyl)-cis-5,6-dipropyl-perhydro-1,3-oxazin-1-one

: 3-((R)-(-)-1-cyclohexylethyl)-cis-5,6-dipropyl-perhydro-1,3-oxazin-1-one

Guidance literature:: N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine; With trifluorormethanesulfonic acid; tetrabutylammonium tetrafluoroborate; In dichloromethane; at -78 ℃; Electrolysis;

(Z)-oct-4-ene; In dichloromethane; at -78 - 0 ℃;

With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1246/bcsj.78.1206

Reference yield: 26.0%

: 863559-77-7
N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine

: 110-83-8
cyclohexene

: 3-((R)-(-)-1-cyclohexylethyl)-5,6-cis-tetramethyleneperhydro-1,3-oxazin-1-one

: 3-((R)-(-)-1-cyclohexylethyl)-5,6-cis-tetramethyleneperhydro-1,3-oxazin-1-one

Guidance literature:: N-(methoxycarbonyl)-N-(trimethylsilylmethyl)-(R)-(-)-1-cyclohexylethylamine; With trifluorormethanesulfonic acid; tetrabutylammonium tetrafluoroborate; In dichloromethane; at -78 ℃; Electrolysis;

cyclohexene; In dichloromethane; at -78 - 0 ℃;

With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1246/bcsj.78.1206